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lab manuals

Experiments in Electroanalytical Chemistry

This website offers educators a set of eight classical electroanalytical experiments suitable for use in a quantitative analysis, instrumental analysis, or electrochemistry course. The materials should be useful for advanced undergraduates and beginning graduate students. Experiments include coulometric, conductometric, and potentiometric titrations, stripping analysis, flow injection analysis, and polarography. The experiments are designed around a common…

Analytical Electrochemistry: A Laboratory Manual

This labware module contains directions for seven experiments in analytical electrochemistry. The experiments are designed to illustrate fundamentals of electrode reactions as applied to readily accessible redox reactants. They provide insight to dynamic electrochemistry for scientists at all levels of training. Activation procedures to prepare glassy carbon electrodes are provided in a TechNote. The website is available…

NMR Spectroscopy: Lab 8

A complete NMR laboratory exercise from a set of fifteen (15) experiments in various topic areas developed for a physical chemistry laboratory at New Mexico State University. Excellent introductory material is provided, along with links to additional sources of information, including NMR tutorials. Pre-lab questions are presented along with detailed laboratory procedures. The two part experiment…

The Evolution of a Laboratory Syllabus for Quantitative Analysis

The paper contains a syllabus of a redesigned quantitative analysis lab. In its new form, the lab is almost entirely instrumental. The description has sufficient detail to assist a fellow instructor to adopt the experiments. A rationale for the experiments and the lab protocols has also been provided.The website is available here .
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