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NMR Spectroscopy: Lab 8

A complete NMR laboratory exercise from a set of fifteen (15) experiments in various topic areas developed for a physical chemistry laboratory at New Mexico State University. Excellent introductory material is provided, along with links to additional sources of information, including NMR tutorials. Pre-lab questions are presented along with detailed laboratory procedures. The two part experiment has students first measure proton spectra for a set of unknown substances and to match the spectra with the compound in a list provided, followed by a kinetics measurement. While the procedure is specific to Varian instruments, users should be able to easily modify the parameters to their own instrument. Site authorization is required to use some of the embedded links, but even without that access, this experiment should be of interest to instructors in both instrumental or physical chemistry.

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